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Distance evaluation via heteronuclear SQC-NOESY experiments |
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| Authors: | Henriette Molinari Gennaro Esposito Roberto Consonni Monica Pegna Lucia Zetta |
| Affiliation: | (1) Dipartimento di Chimica Organica e Industriale, Università di Milano, Via Golgi 19, 20133 Milano, Italy;(2) Istituto di Biologia, Università degli Studi di Udine, Via Gervasutta 48, 33100 Udine, Italy;(3) Laboratorio NMR, Istituto di Chimica delle Macromolecole del CNR, Via Ampere 56, 20131 Milano, Italy;(4) ITALFARMACO c/o Laboratorio NMR, Istituto Chimica delle Macromolecole del CNR, Via Ampere 56, 20131 Milano, Italy |
| Abstract: | Summary A method for the quantitative determination of interproton distances from1H NOE relayed heteronuclear correlation is presented. Model compounds are investigated. Accurate distances are obtained if all the factors affecting such distance measurements, such as the local mobility and the presence of strong coupling in heteronuclear systems, are properly taken into account. |
| Keywords: | Distance evaluation SQC-NOESY NMR Heteronuclear |
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