| 羧基化聚丙烯酸酯接枝邻甲酚环氧丙烯酸树脂的合成 |
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| 引用本文： | 黎文部,王洛礼,于洁. 羧基化聚丙烯酸酯接枝邻甲酚环氧丙烯酸树脂的合成[J]. 武汉生物工程学院学报, 2006, 0(1) |
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| 作者姓名： | 黎文部 王洛礼 于洁 |
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| 作者单位： | 武汉生物工程学院应用化学系 湖北武汉430415(黎文部)，湖北省化学研究院 湖北武汉430074(王洛礼，于洁) |
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| 基金项目： | 国家863计划资助项目(2004AA001300) |
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| 摘 要： | 采用JF-220环氧树脂和丙烯酸反应合成邻甲酚环氧丙烯酸树脂(JFA),再将其和羧基化聚丙烯酸酯进一步反应制备羧基化聚丙烯酸酯接枝邻甲酚环氧丙烯酸树脂(CAJFA)。研究了催化剂、阻聚剂和反应温度对合成反应的影响,确定了每步反应的最佳合成条件,并且对JF-220树脂、JFA树脂和CAJFA树脂的结构进行了IR表征。
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| 关 键 词： | 各向异性导电胶粘剂膜 羧基化聚丙烯酸酯 邻甲酚环氧丙烯酸树脂 |
Synthesis of Carboxylated Polyacrylate Grafted Cresol Novolac Epoxy Acrylate Resin |
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| LI Wenbu WANG Luoli YU Jie. Synthesis of Carboxylated Polyacrylate Grafted Cresol Novolac Epoxy Acrylate Resin[J]. Journal of Wuhan Bioengineering Institute, 2006, 0(1) |
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| Authors: | LI Wenbu WANG Luoli YU Jie |
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| Abstract: | Cresol novolac epoxy acrylate resin(JFA)was synthesized by JF-220 epoxy resin with acrylic acid,and then carboxylated polyacrylate grafted cresol novolac epoxy acrylate resin(CAJFA)was pre- pared by JFA with carboxylated polyacrylate.The effects of catalysts,inhibitors and reactive tempera- ture on the reaction were studied and the best synthetic conditions of each step were determined.Struc- tures of JF-220,JFA and CAJFA resins were characterized by IR spectrometer. |
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| Keywords: | anisotropic conductive adhesives film carboxylated polyacrylate o-cresol (2-methylphenol) novolac epoxy acrylate resin |
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