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HS-SPME & GC-MS分析印加果种子的挥发性物质
引用本文:陈鸿鹏,彭彦,林彦,高丽琼,吴志华,李慧,谢耀坚.HS-SPME & GC-MS分析印加果种子的挥发性物质[J].亚热带植物科学,2015,44(3):199-203.
作者姓名:陈鸿鹏  彭彦  林彦  高丽琼  吴志华  李慧  谢耀坚
作者单位:(国家林业局桉树研究开发中心,广东 湛江 524022)
基金项目:广东省林业科技创新项目(2011KJCX019, 2014KJCX016-03);湛江市科技计划项目(2014A03013);引进国际先进林业科学技术“948”项目(2014-4-21)
摘    要:利用顶空固相微萃取-气相色谱质谱法(HS-SPME & GC-MS)分析印加果Plukenetia volubilis近成熟种子的挥发性物质,通过面积归一法计算出各成分的相对含量。结果共分离鉴定出64种化学成分,其中6种酯类化合物,占45.86%;12种醇类化合物,占27.71%;7种烯烃类化合物,占6.71%;9种醛类化合物,占3.89%;6种酮类化合物,占2.78%;16种烷烃类化合物,占1.78%。此外,盐酸氨基脲占5.47%,氨基脲占3.25%,还有1.51%三氯乙酸和0.23%甲基异丙基苯及其他化合物。

关 键 词:HS-SPME  &GC-MS  印加果  种子  挥发性物质  
收稿时间:2015-05-11
修稿时间:2015-11-26

Analysis of Volatile Components from Plukenetia volubilis Seed by HS-SPME & GC-MS
CHEN Hong-peng,PENG Yan,LIN Yan,GAO Li-qiong,WU Zhi-hua,LI Hui,XIE Yao-jian.Analysis of Volatile Components from Plukenetia volubilis Seed by HS-SPME & GC-MS[J].Subtropical Plant Science,2015,44(3):199-203.
Authors:CHEN Hong-peng  PENG Yan  LIN Yan  GAO Li-qiong  WU Zhi-hua  LI Hui  XIE Yao-jian
Institution:(China Eucalypt Research Center, Zhanjiang 524022, Guangdong China)
Abstract:In order to reveal the aroma characteristics of Sacha Inchi seed oil, volatile components from nearly-matured seed of Sacha Inchi were analyzed by HS-SPME & GC-MS and the relative content of each component was determinated by area normalization. The results showed that 64 chemical composition were detected and identified including 6 ester compounds (45.86%), 12 alcohol compounds (27.71%), 7 alkene compounds (6.71%), 9 aldehyde compounds (3.89%), 6 ketone compounds (2.78%) and 16 alkane compounds (1.78%). Moreover, semicarbazide hydrochloride (5.47%), hydrazine carboxamide (3.25%), trichloro-acetic acid (1.51%), methyl(1-methylethyl)-benzene (0.23%) and others were also identified.
Keywords:HS-SPME &GC-MS  Plukenetia volubilis  seed  volatile component  
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