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Simple, inexpensive attainment and measurement of very high cooling and warming rates
Authors:F.W. Kleinhans  Shinsuke Seki
Affiliation:a Fundamental and Applied Cryobiology Group, Department of Biochemistry and Cellular and Molecular Biology, The University of Tennessee, Knoxville, TN 37932, USA
b Department of Physics, IUPUI, Indianapolis, IN 46202, USA
Abstract:We have developed a simple, inexpensive system (<$300 US) for measuring cooling and warming rates of small (∼ 0.1 μl) aqueous samples at rates as high as 105 °C/min. The measurement system itself, can track rates approaching one million °C/min. For temperature sensing, a Type T thermocouple with 50 μm wire was used. The thermocouple output voltage was read with an inexpensive USB based digital oscilloscope interfaced to a laptop computer, and the raw data were processed with MS Excel.
Keywords:Inexpensive temperature measurement   High rate   Warming   Cooling   Type T thermocouple   USB oscilloscope   Cryotop
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