Applications of chromic acid-Celite columns to micro- and semimicro preparations of fatty aldehydes. |
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Authors: | D P Schwartz S F Osman |
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Institution: | Eastern Regional Research Center, Philadelphia, Pennsylvanla 191181 USA |
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Abstract: | In a convenient two-phase procedure, columns of Celite 545 charged with aqueous chromic acid are used to oxidize microgram and milligram amounts of fatty alcohols to the corresponding aldehydes with approximately a 70% yield. The original configuration and position of the double bond is fully maintained during the oxidation of unsaturated alcohols. |
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