A 13c-n.m.r. study of a di- and a tri-saccharide containing the α-d-galactopyranosyl group |
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Authors: | Daniel D Cox E Kurt Metzner Lewis W Cary Elmer J Reist |
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Institution: | SRI International, Menlo Park, California 94025 U.S.A. |
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Abstract: | The 13C-n.m.r. spectra of methyl 4-O-α-d-galactopyranosyl-α-d-galactopyranoside (1) and methyl 4-O-4-O-(α-d-galactopyranosyl)-β-d-galactopyranosyl]-β-d-glucopyranoside (2) in D2O were recorded. Comparison of these spectra with the spectra of methyl α-d-galactopyranoside (4) and methyl β-lactoside (5) provided substantial confirmation of the structures of 1 and 2. |
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