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A convenient synthesis of glycosyl chlorides from sugar hemiacetals using triphosgene as the chlorine source |
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| Authors: | Cicchillo R M Norris P |
| Affiliation: | Department of Chemistry, Youngstown State University, OH 44555-3663, USA. |
| Abstract: | Treating partially protected sugar hemiacetals with triphosgene in THF results in the formation of glycosyl chlorides. The method is compatible with acid-sensitive isopropylidene protecting groups in the hemiacetal substrates. |
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