| 北青龙衣质量控制的研究 |
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| 引用本文： | 刘丽娟,张丽杰,张华.北青龙衣质量控制的研究[J].现代生物医学进展,2010,10(2). |
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| 作者姓名： | 刘丽娟 张丽杰 张华 |
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| 作者单位： | 黑龙江大学制药工程系,黑龙江,哈尔滨,150080 |
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| 基金项目： | 黑龙江省科技厅青年科技创新基金(QC07C65); 黑龙江省教育厅青年基金(11531279); 哈尔滨市科技局科技创新人才研究专项基金(2008RFQXS106) |
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| 摘 要： | 目的:建立北青龙衣质量控制的方法。方法:采用薄层色谱进行鉴别,展开条件为三氯甲烷-甲醇(8:2),采用高效液相色谱进行含量测定,以乙腈-水-磷酸(10:90:0.2)为流动相,指标成分为(4S)-4,5-二羟基-α-四氢萘酮-4-O-β-D-吡喃葡糖苷。结果:方法灵敏、可靠、准确、重复性好。结论:该方法可作为北青龙衣质量控制的方法。
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| 关 键 词： | 北青龙衣 薄层色谱 含量测定 质量控制 |
Study on the Quality Control of the Fresh Rejuvenated Fruits of Juglans Mandshurica |
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| LIU Li-juan,ZHANG Li-jie,ZHANG Hua.Study on the Quality Control of the Fresh Rejuvenated Fruits of Juglans Mandshurica[J].Progress in Modern Biomedicine,2010,10(2). |
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| Authors: | LIU Li-juan ZHANG Li-jie ZHANG Hua |
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| Institution: | ZHANG Li-jie,ZHANG Hua,LIU Li-juan(Department of Pharmacy of Heilongjiang University,Harbin 150080,China) |
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| Abstract: | Objective:To establish the method of quality control of the fresh rejuvenated fruits of J. mandshurica. Methods:The identification was achieved by TLC and the solvent was CHCl3-MeOH(8:2) . The content determination was achieved by HPLC and elution condition was MeCN-H2O-H3PO4(10:90:0.2) . The marker component was(4S) -4,5-dihydroxy-tetralone 4-O-D-glucopyranoside. Results:The method is sensitive,reliable,accurate and repeatability. Conclusions:It can be used for quality control of the fresh rejuvenated frui... |
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| Keywords: | the fresh rejuvenated fruits of J mandshurica TLC HPLC quality control |
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