Determination of beta-carboline alkaloids in fruiting bodies of Hygrophorus spp. by liquid chromatography/electrospray ionisation tandem mass spectrometry |
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Authors: | Teichert Axel Lübken Tilo Schmidt Jürgen Kuhnt Christine Huth Manfred Porzel Andrea Wessjohann Ludger Arnold Norbert |
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Affiliation: | Department of Bioorganic Chemistry, Leibniz Institute of Plant Biochemistry, Weinberg 3, 06120 Halle (Saale), Germany. |
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Abstract: | The beta-carboline alkaloids harmane (1) and norharmane (2) were isolated from fruiting bodies of Hygrophorus eburneus (Bull.) Fr. as well as brunnein A (3) from Hygrophorus hyacinthinus Quél. (Tricholomataceae, Agaricales) for the first time. Their occurrence within the genus was investigated using liquid chromatography/electrospray ionisation tandem mass spectrometric methods, especially by selected reaction monitoring. Based on these results their chemotaxonomical relevance is discussed. |
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Keywords: | LC/ESI‐SRM harmane norharmane brunnein A Hygrophorus Basidiomycetes |
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