Rapid synthesis of long chain fatty acid esters of steroids in ionic liquids with microwave irradiation: Expedient one-pot procedure for estradiol monoesters |
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Authors: | Somdatta Deb |
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Affiliation: | Laboratory of Organic Chemistry, University of Helsinki, A.I. Virtasen aukio 1, POB 55, FIN-00014 Helsinki, Finland |
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Abstract: | We report the rapid synthesis (1 min) in high yield of fatty acid ester (FAE) derivatives of several steroids under microwave irradiation in an ionic liquid (IL). An expedient regioselective hydrolysis at C-3 of estradiol diesters is also reported. |
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Keywords: | Microwave Ionic liquid Estradiol DHEA Testosterone 5α-Androstane-3β,17β-diol |
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