Single-flask synthesis of (C5H5)W(CO)3Cl from W(CO)6 |
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Authors: | Norris W Hoffman |
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Institution: | Union Carbide Corporation, P.O. Box 8361, South Charleston, W.V. 25303, U.S.A. |
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Abstract: | (C5H5)W(CO)3Cl has been prepared in >90% yield from W(CO)6, cyclopentadiene, and CCl4 in a single-flask synthesis involving the intermediates W(CO)3(CH3CN)3 and (C5H5)W(CO)3H. |
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