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Gas-liquid chromatographic analysis of diglycerides
Authors:J F O'Brien  W E Klopfenstein
Affiliation:1. Laboratorio de Investigación y Desarrollo en Métodos Analíticos (LIDMA)-CIC-PBA, Facultad de Ciencias Exactas, Universidad Nacional de La Plata (UNLP), Calle 49 y 115 (B1900AJL), La Plata, Argentina;2. División Química Analítica, Facultad de Ciencias Exactas, Universidad Nacional de La Plata, (UNLP), 47 y 115 (B1900AJL), Ciudad de La Plata, Provincia de Buenos Aires, Argentina;1. Engineering Research Center of Pharmaceutical Process Chemistry, Ministry of Education, School of Pharmacy, East China University of Science and Technology, Shanghai 200237, PR China;2. Key Lab of Separation Science for Analytical Chemistry, Key Lab of Natural Medicine, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, Liaoning 116023, PR China;1. State Key Laboratory for Managing Biotic and Chemical Threats to the Quality and Safety of Agro-products, State Key Laboratory Base of Novel Functional Materials and Preparation Science, School of Materials Science & Chemical Engineering, Ningbo University, Ningbo, Zhejiang, 315211, China;2. Healthy & Intelligent Kitchen Engineering Research Center of Zhejiang Province, Ningbo, Zhejiang, China
Abstract:A gas-liquid chromatography method for the resolution of 1,2-diglycerides of a given carbon number from the 1,3-isomers of the same carbon number is presented. Resolution of saturated diglycerides from the unsaturated diglycerides is also achieved, although complete resolution of unsaturated diglycerides is not obtained.
Keywords:
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