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硬毛地笋挥发性成分研究
引用本文:彭涛,王金梅,张前军,康文艺. 硬毛地笋挥发性成分研究[J]. 天然产物研究与开发, 2012, 24(3): 342-344
作者姓名:彭涛  王金梅  张前军  康文艺
作者单位:1. 河南大学药学院中药研究所,开封475004;贵州大学化学化工学院,贵阳550025;贵州大学精细化工研究开发中心,贵阳550025
2. 河南大学药学院中药研究所,开封,475004
3. 贵州大学化学化工学院,贵阳,550025
4. 河南大学药学院中药研究所,开封475004;贵州大学化学化工学院,贵阳550025
摘    要:采用固相微萃取/气相色谱/质谱法对硬毛地笋地上部分挥发油成分进行分离和鉴定。首次从硬毛地笋地上部分中鉴定出了20个化合物,占总挥发性成分的98.68%。主要挥发性成分为石竹烯(30.87%)、(–)-α-人参烯(11.56%)、佛术烯(9.38%)、Z,Z,Z-1,5,9,9-四甲基-1,4,7,-环十一碳三烯(9.10%)、2-异丙基甲苯(5.65%)、大牛儿烯D(4.34%)、D-柠檬烯(3.95%)和γ-瑟林烯(3.79%)。

关 键 词:硬毛地笋  挥发油  HS-SPME-GC-MS

Volatile Oils Constituents of Lycopus lucidus var.hirtus
PENG Tao , WANG Jin-mei , ZHANG Qian-jun , KANG Wen-yi. Volatile Oils Constituents of Lycopus lucidus var.hirtus[J]. Natural Product Research and Development, 2012, 24(3): 342-344
Authors:PENG Tao    WANG Jin-mei    ZHANG Qian-jun    KANG Wen-yi
Affiliation:1,2* 1Institute of Chinese Materia Medica,Pharmaceutical College,Henan University,Kaifeng 475004,China; 2School of Chemistry and Chemical Engineer of Guizhou University; 3Research and Development Center of Fine Chemicals of Guizhou University,Guiyang 550025,China
Abstract:The constituents of volatile oils of Lycopus lucidus var.hirtus were analyzed by head-space solid micro-extraction,coupled with GC-MS.Twenty compounds were identified from the L.lucidus var.hirtus for the first time and account for 98.68% of the total volatiles.The main compounds were caryophyllene(30.87%),(–)-α-panasinsen(11.56%),eremophilene(9.38%),Z,Z,Z-1,5,9,9-tetramethyl-1,4,7-cycloundecatriene(9.10%),2-cymene(5.65%),germacrene D(4.34%),D-limonene(3.95%) and γ-selinene(3.79%).
Keywords:Lycopus lucidus var.hirtus  volatiles oils  HS-SPME-GC-MS
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