The synthesis of cholesteryl alkyl ethers |
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| Authors: | G. Halperin S. Gatt |
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| Affiliation: | 1. Lipid Research Laboratory, Department of Medicine B, Hadassah University Hospital Israel;2. Department of Biochemistry, Hebrew University-Hadassah Medical School, Jerusalem, Israel |
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| Abstract: | Seventeen cholesteryl alkyl ethers were synthesized through alcoholysis of cholesterol p-toluenesulfonate. This method was found superior to the etherification of sodium or potassium cholesterylate with alkyl halides or methanesulfonates, especially for the preparation of long-chain unsaturated alkyl ethers of [7(n)-3H]cholesterol of high specific activity. |
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