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A simple method of determining zearalenone in cereals by liquid chromatography
Authors:K Kallela  I Saastamoinen
Institution:(1) Department of Animal Hygiene, College of Veterinary Medicine, Helsinki, Finland
Abstract:Summary The paper described a simplified method for the separation, identification and determination of zearalenone by liquid chromatography in cereals. The cereal medium is dried, homogenised and extracted with ether. From the ether extract zearalenone is transferred into ethyl acetate, whereafter the sample is analysed using an external standard. The detection limit of the method is 500 mgrg/kg. Recoveries of zearalenone varied from 94.5% to 96.2%.The conditions of the liquid chromatography are described.
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