紫芝超细粉挥发油成分GC-MS分析 |
| |
引用本文: | 陈体强,吴锦忠,朱金荣.紫芝超细粉挥发油成分GC-MS分析[J].菌物学报,2007,26(2):279-283. |
| |
作者姓名: | 陈体强 吴锦忠 朱金荣 |
| |
作者单位: | 1. 福建省农业科学院,福州,350013 2. 福建中医学院药学系,福州,350003;福州大学化学与化工学院,福州,350012 3. 福州大学化学与化工学院,福州,350012 |
| |
基金项目: | 福建省自然科学基金
,
福建省科技计划 |
| |
摘 要: | 将紫芝Ganoderma sinense(“闽紫96”,HMAS 77207,阔叶树枝桠材或边材栽培)超微粉碎加工成500目的子实体超细粉。激光粒度分析表明:紫芝超细粉的表面积到834.18m~2/kg,中位径(D50)为12.68μm。气质联用分析结果表明:从紫芝超细粉挥发油中分离到35种成分,出峰时间为7.872~30.239min,确定了其中32个成分,占相对含量的88.642%;绝大多数成分为脂肪族化合物(67.216%),主要成分(20.67%)为2,6-二叔丁基一苯酚为芳香族化合物,还检出2种杂环族化合物。
|
关 键 词: | 紫芝 超细粉 挥发油 化学成分 |
文章编号: | 1672-6472(2007)02-0279-0283 |
收稿时间: | 2006-07-30 |
修稿时间: | 2006-07-302006-09-10 |
GC-MS analysis of chemical components in the essential oils of from the ultrafine-powder of Ganoderma sinense |
| |
Authors: | CHEN Ti-Qiang WU Jin-Zhong and ZHU Jin-Rong |
| |
Institution: | Fijian Academy of Agricultural Sciences, Fuzhou 350013;(2.Department of TCM Pharmacology, Fujian College of Traditional Chinese Medicine, Fuzhou 350013);(3.College of Chemistry & Chemical Engineering, Fuzhou University, Fuzhou 350012);College of Chemistry & Chemical Engineering, Fuzhou University, Fuzhou 350012 |
| |
Abstract: | The fruitbodies of Ganoderma sinense(“Minzi 96”strain,HAMS 77207,cultivated with laburnum or branches of broadleaf tree)were processed into ultrafine-powder that sifted throughΦ500 R40/3 sieve.And the granularity were tested by laser grain-size analysis,that specific surface area(BET)was 834.18m~2/kg,and the cumulative distribution data D50 was 12.68μm(equivalent grain-size).35 compositions of total essential oil from the ultrafine-powder were separated and identified by GC-MS,retention time arranged from 7.872 min to 30.239min.The results indicated that 32 compounds were determinated,and their relative contents were about 88.64%,most of the compounds belong to aliphatic compounds(67.216%),and the main constituent with highest relative content(20.67%)have been identified as 2,6-di-tert-butylphenol(aromatics compounds),moreover,two compounds of heterocyclics were also checked out. |
| |
Keywords: | Ganoderma sinense ultra-fine powder esstional oil chemical component |
本文献已被 CNKI 维普 万方数据 等数据库收录! |
| 点击此处可从《菌物学报》浏览原始摘要信息 |
| 点击此处可从《菌物学报》下载免费的PDF全文 |
|