Complete analysis of the1H- and13C-NMR spectra of four blood-group A active oligosaccharides |
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| Authors: | Gérard Strecker Jean-Michel Wieruszeski Jean-Claude Michalski Jean Montreuil |
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| Institution: | Laboratoire de Chimie Biologique, Université des Sciences et Techniques de Lille Flandres-Artois, Villeneuve d'Ascq, France. |
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| Abstract: | The fully assigned 1H and 13C-NMR spectra of four group A oligosaccharides by use of multiple-relayed, coherence-transfer chemical-shift-correlated spectroscopy (multiple-RELAY-COSY) and 1H-/13C-correlation spectroscopy are reported. These analyses were performed on the following compounds: III-A; GalNAc alpha 1-3Fuc alpha 1-2]Gal: VI-A; GalNAc alpha 1-3Fuc alpha 1-2]Gal beta 1-3Fuc alpha 1-4]GlcNAc beta 1-3Gal: VII-A-1; GalNAc alpha 1-3Fuc alpha 1-2]Gal beta 1-3Fuc alpha 1-4]GlcNAc beta 1-3Gal beta 1-1Glycerol: VII-A-2; GalNAc alpha 1-3Fuc alpha 1-2]Gal beta 1-3Fuc alpha 1-4]GlcNAc beta 1-3Gal beta 1-4Glc. |
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