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| 微滤膜分离提纯苦楝素的研究 | |
| 引用本文： | 王龙德,崔鹏,路绪旺,佟玲,姚路路. 微滤膜分离提纯苦楝素的研究[J]. 天然产物研究与开发, 2011, 23(4): 742-746 |
| 作者姓名： | 王龙德 崔鹏 路绪旺 佟玲 姚路路 |
| 作者单位： | 1. 淮南师范学院化学与化工系,淮南,232001 2. 合肥工业大学化工学院安徽省可控化学与材料化工重点实验室,合肥,230009 3. 淮南师范学院化学与化工系,淮南232001; |
| 基金项目： | 安徽省高等学校科研项目 |
| 摘 要： | 通过对不同孔径和材质的微孔滤膜对苦楝提取液过滤分离比较,优选出孔径为0.45μm的聚醚砜微滤膜对苦楝提取液具有良好的过滤性能。确定的膜分离提纯苦楝素优化工艺条件是:在料液浓度为0.374 mg/mL,料液温度35℃,操作压力差为0.08 MPa,循环流量为0.15 L/h,pH=7.0,苦楝素的转移率为99.4%,除杂率为8.3%,通量为147.2 L/m2.h,苦楝素的纯度为由提取液的0.89%,提高到了8.79%。 |
| 关 键 词： | 苦楝 苦楝素 膜分离 提纯 |
Separation and Purification of Toosendanin Extraction Solution by Microfiltration Membrane Technology |
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| WANG Long-de,CUI Peng,LU Xu-wang,TONG Ling,YAO Lu-lu. Separation and Purification of Toosendanin Extraction Solution by Microfiltration Membrane Technology[J]. Natural Product Research and Development, 2011, 23(4): 742-746 | |
| Authors: | WANG Long-de CUI Peng LU Xu-wang TONG Ling YAO Lu-lu |
| Affiliation: | WANG Long-de1,CUI Peng2,LU Xu-wang2,TONG Ling1,YAO Lu-lu2 1Department of Chemistry and Chemical Engineering,Huainan Normal College,Huainan 232001,China,2School of Chemical Engineering,Hefei University of Technology,Anhui Key laboratory of Controllable Chemical Reaction & Material Chemical Engineering,Hefei 230009 |
| Abstract: | The experimental study of toosendanin enrichment from extracts of Melia azedarach by membrane filtration was performed using polyethersulfone microfiltration membrane with average pore size of 0.45 μm.Under optimized concentration of 1.134 mg/mL,pH = 7.0,circulation flow rate 0.15 L/h,operating pressure of 0.08 MPa,temperature 35 ℃,the toosendanin transfer rate was 99.4% with 8.3% impurity decrease.Microfiltration flux reached up to 147.2 L/m2·h and toosendanin concentration increased from 0.89% to 8.79%. |
| Keywords: | Melia azedarach toosendanin membrane separation purification |
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