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Solvent-free synthesis of glyceryl ferulate using a commercial microbial lipase
Authors:Shangde Sun  Liang Shan  Qingzhe Jin  Yuanfa Liu  Xingguo Wang
Affiliation:(1) School of Food Science and Technology, Southern Yangtze University, The Key Laboratory of Food Science and Safety, Ministry of Education, 170 Huihe Road, Wuxi, 214036, Jiangsu, P.R. China
Abstract:A process was optimized for the enzymatic synthesis of glyceryl ferulate with a yield of up to 96% using a vacuum-rotary evaporation strategy under following conditions: 15 mmol glycerol, 1.5 mmol ethyl ferulate, 170 mg Candida antarctica lipase, at 60°C for 10 h and under a vacuum of 10 mm Hg. The immobilized lipase can be used 10 times.
Keywords:Candida antarctica lipase  Ethyl ferulate  Glyceryl ferulate  Solvent-free synthesis  Transesterification
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