Solvent-free synthesis of glyceryl ferulate using a commercial microbial lipase |
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Authors: | Shangde Sun Liang Shan Qingzhe Jin Yuanfa Liu Xingguo Wang |
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Affiliation: | (1) School of Food Science and Technology, Southern Yangtze University, The Key Laboratory of Food Science and Safety, Ministry of Education, 170 Huihe Road, Wuxi, 214036, Jiangsu, P.R. China |
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Abstract: | A process was optimized for the enzymatic synthesis of glyceryl ferulate with a yield of up to 96% using a vacuum-rotary evaporation strategy under following conditions: 15 mmol glycerol, 1.5 mmol ethyl ferulate, 170 mg Candida antarctica lipase, at 60°C for 10 h and under a vacuum of 10 mm Hg. The immobilized lipase can be used 10 times. |
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Keywords: | Candida antarctica lipase Ethyl ferulate Glyceryl ferulate Solvent-free synthesis Transesterification |
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