Research of the Dispersity of the Functional Sericite/Methylphenyl- Silicone Resin |
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| Authors: | B. Jiang C. C. Zhu Y. D. Huang |
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| Affiliation: | 1. State Key Laboratory of Urban Water Resource and Environment, Harbin Institute of Technology, Harbin 150090.; 2. Polymer Materials and Engineering Department, School of Chemical Engineering and Technology, Harbin Institute of Technology, P.O. Box: 1254, Harbin 150001, People’s Republic of China.; Bascom Palmer Eye Institute, University of Miami School of Medicine, UNITED STATES, |
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| Abstract: | In order to improve the homogeneity and dispersity of the sericite in methylphenyl-silicone resin, the agglomerate state of the sericites was controlled effectively. The dispersive model of the sericite in methylphenyl-silicone resin was designed also. First, the modified sericite was prepared using hexadecyl trimethyl ammonium bromide as the intercalating agent. Then, functional sericite was incorporated into methylphenyl-silicone by terminal hydroxyl. The structure and dispersive performance of the hybrid polymers was charactered by analytical instruments. Scanning electron microscopy and Transmission electron microscope, Laser scanning confocal microscope and X-ray diffraction analysis showed that functional sericite was dispersed homogeneously in methylphenyl-silicone resin matrix. X-ray photoelectron spectroscopy analysis showed that the absorption peaks of the Si-OH band of methylphenyl-silicone resin were decreased and the Si-O-Si band was increased. This change evidently showed a significant role to enhance the reaction degree of the functional sericite in methylphenyl-silicone resin. |
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