共查询到18条相似文献,搜索用时 78 毫秒
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从匙叶八角(Illicium spathulatum)果实中分离得到一个新的倍半新木脂素,通过现代波谱技术确定其结构为7′, 8′-反式-7″, 8″ 顺式-5, 3′,3″-三甲氧基倍半新木脂素。 相似文献
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为了解青阳参(Cynanchum otophyllum Schneid)根的酸催化水解物化学成分.利用硅胶柱色谱、ODS、HPLC等多种柱色谱分离手段对青阳参95%乙醇提取物的酸催化水解物进行了分离纯化,从中得到了4个木脂素,通过波谱学方法鉴定其结构,分别为9'-methoxynegundin B(1)、(+)-iso... 相似文献
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长缘厚朴中的新苯醌及新木脂素类化合物 总被引:8,自引:2,他引:6
从长缘厚朴(Magnolia rostrata W.W.Smith)树皮中分离得到1个新化合物-联烯丙基苯对苯醌类物质,命名为木兰醌magnoquinone(1),以及7个已知新木脂素类化合物,厚朴酚magnolol(2),和厚朴酚honokiol(3),4-o-methylhonokiol(4),3-o-methylmagnolol(5),magnoldehydeB(6),magnolignanA(7)和magnolignanC(8)。研究表明,长缘厚扑可作为中药厚朴(Magnolia officinalis)的代用品。 相似文献
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云南铁杉中一个新的倍半木脂素 总被引:1,自引:1,他引:0
从云南铁杉(Tsuga dumosa) 心材中分离得到9 个化合物, 采用波谱方法鉴定了它们的结构。其中化合物1 (3 (4 hydroxy 3 methoxy benzyl ) 5 [2 (4 hydroxy 3 methoxy phenyl ) 3 hy droxymethyl 7 methoxy 2, 3 dihydro benzofuran 5 yl] 4 hydroxymethyl dihydro furan 2 one) 为一个新的倍半木脂素, 命名为dumosaol, 2~9为首次从该种植物中分离得到。 相似文献
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红蓼中木脂素成分的研究 总被引:8,自引:0,他引:8
从红蓼(PolygonumorientaleL.)中分得3个木脂素类化合物,经光谱分析和化学方法鉴定为牛蒡子甙(1)、拉帕酚B(2)和红蓼脂素(3)。其中化合物3为新化合物,1和2为首次从该植物中分离得到。 相似文献
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《Bioscience, biotechnology, and biochemistry》2013,77(4):878-881
The optically active samin type of lignan, (1R,2S,5R, 6S)-6-(2-methoxy-4,5-methylenedioxyphenyl)-3,7-dioxabicyclo[3.3.0]octan-2-ol, was stereoselectively synthesized from L-glutamic acid via (2R,3R)-2-[(1S and R)- 1-[(tert-butyldimethylsilyl)oxy]-1-(2-methoxy-4,5-methylenedioxyphenyl)methyl]-3-[(tert-butyldiphenylsilyl)oxy]methyl-1,4-butanediol. 相似文献
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《Bioscience, biotechnology, and biochemistry》2013,77(8):1563-1571
The olivil type of lignan, (2S,3R,4R)-4-benzyl-4- hydroxy-3-hydroxymethyl-2-(3,4-methylenedioxyphenyl)tetrahydrofuran, was stereoselectively synthesized from D-xylose. 相似文献
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《Bioscience, biotechnology, and biochemistry》2013,77(10):2144-2147
The new lignan glucoside, acutumoside (1), was isolated from Sinomenium acutum rhizomes together with nine known compounds (2–10). The structure of 1 was elucidated on the basis of extensive spectroscopic analyses, including two-dimensional nuclear magnetic resonance and chemical reactions. Compounds 2, 7, 8, and 10 displayed potential antiproliferative activity against A549, SK-OV-3, SK-MEL-2, and HCT-15 cell lines, while compound 1 showed weak activity against these human tumor cells. 相似文献
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从狭基线纹香茶菜 (Isodonlophanthoidesvar.gerardianus [Bentham]H .Hara)的乙酸乙酯部分分离得到两个木脂素类化合物 ,经 1D、2D_NMR技术鉴定 ,分别为 1_acetoxyl_2e,6e_dipiperonyl_3,7_dioxabicyclo_[3,3,0 ]_octane (1)和 1_acetoxyl_2e_piperonyl_6e_[6_methoxyl_piperonyl]_3,7_dioxabicyclo_[3,3,0 ]_octane (2 ) ,其中 2为新化合物。 相似文献
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《Bioscience, biotechnology, and biochemistry》2013,77(7):1238-1241
The new lignan derivative, erimopyrone, was isolated from the liverwort, Moerckia erimona. Its structure was established as [1R, 2S]-1(6-carboxy-2-oxo-2H-4-pyranyl)- 6,7-dihydroxy-1,2-dihydro-2,3-naphthalenedicarboxylic acid by spectroscopic methods. 相似文献
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《Bioscience, biotechnology, and biochemistry》2013,77(7):1559-1567
(+)-Magnostellin C, which is a tetrahydrofuran type of lignan bearing a chiral secondary benzylic hydroxy group, was stereoselectively synthesized from L-arabinose by using threo selective aldol condensation. 相似文献
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《Bioscience, biotechnology, and biochemistry》2013,77(8):1718-1721
The inhibitory effect of (?)-, (+)-matairesinol and (?)-, (+)-secoisolariciresinol on the discoloration of dark muscle (chiai in Japanese) of two-year-old yellowtail (hamachi in Japanese) was evaluated by measuring the X and a* values. (?)-Matairesinol was most effective for retaining the red color of dark muscle in this experiment. 相似文献