安徽省和县和巢县古人类地点的铀系法年代测定和研究

用不平衡铀系法测定了安徽省和县和巢县人化石地点哺乳动物骨化石样品的年代。所得封闭样品的年代值分别集中在15—19和16—20万年范围内。但在两个地点均不排除年代值为二十多万年的骨化石样品存在的可能。所有被测样品均检验了对铀的封闭性。     

26Al/10Be Burial Dating of Xujiayao-Houjiayao Site in Nihewan Basin,Northern China

The Xujiayao-Houjiayao site in Nihewan Basin is among the most important Paleolithic sites in China for having provided a rich collection of hominin and mammalian fossils and lithic artifacts. Based on biostratigraphical correlation and exploratory results from a variety of dating methods, the site has been widely accepted as early Upper Pleistocene in time. However, more recent paleomagnetic analyses assigned a much older age of ∼500 ka (thousand years). This paper reports the application of ²⁶Al/¹⁰Be burial dating as an independent check. Two quartz samples from a lower cultural horizon give a weighted mean age of 0.24 ± 0.05 Ma (million years, 1σ). The site is thus younger than 340 ka at 95% confidence, which is at variance with the previous paleomagnetic results. On the other hand, our result suggests an age of older than 140 ka for the site’s lower cultural deposits, which is consistent with recent post-infrared infrared stimulated luminescence (pIR-IRSL) dating at 160–220 ka.     

Luminescence chronology of cave sediments at the Atapuerca paleoanthropological site, Spain

Ascertaining the timing of the peopling of Europe, after the first out-of-Africa demographic expansion at the end of the Pliocene, is of great interest to paleoanthropologists. One of the earliest direct evidences for fossil hominins in western Europe comes from an infilled karstic cave site called Gran Dolina at Atapuerca, in a stratum approximately 1.5m below the Brunhes-Matuyama (B-M) geomagnetic boundary (780ka) within lithostratigraphic unit TD6. However, most of the meters of fossil- and tool-bearing strata at Gran Dolina have been difficult to date. Therefore, we applied both thermoluminescence (TL) and infrared-stimulated-luminescence (IRSL) multi-aliquot dating methods to fine-silt fractions from sediment samples within Gran Dolina and the nearby Galería cave site. We also applied these methods to samples from the present-day surface soils on the surrounding limestone hill slopes to test the luminescence-clock-zeroing-by-daylight assumption. Within the uppermost 4m of the cave deposits at Gran Dolina, TL and paired TL and IRSL ages range stratigraphically from 198+/-19ka to 244+/-26ka. Throughout Gran Dolina, all luminescence results are stratigraphically self-consistent and, excepting results from two stratigraphic units, are consistent with prior ESR-U-series ages from progressively deeper strata. Thermoluminescence ages culminate at 960+/-120ka approximately 1m below the 780ka B-M boundary. At Galería, with one exception, TL and IRSL ages range stratigraphically downward from 185+/-26ka to 503+/-95ka at the base of the lowermost surface-inwash facies. These results indicate that TL and (sometimes) IRSL are useful dating tools for karstic inwash sediments older than ca. 100ka, and that a more accurate chronostratigraphic correlation is now possible among the main Atapuerca sites (Gran Dolina, Galería, Sima de los Huesos). Furthermore, the oldest TL age of ca. 960ka from Gran Dolina, consistent with biostratigraphic and paleomagnetic evidence, implies a probable numeric age of 900-950ka for the oldest hominin remains ( approximately 0.8m below the TL sample). This age window suggests a correspondence to Marine Isotope Stage (MIS) 25, a relatively warm and humid interglaciation.     

云南西畴仙人洞动物化石铀系年代

本文报道晚期智人地点云南西畴仙人洞动物牙化石的铀系测年结果。4个样品的230Th234U年龄范围为47—105ka,测定了其中2个样品的227Th/230Th年龄,结果与230Th/234U法的一致。在没有进一步的地层和年代证据的情况下,将西畴人牙化石的年代暂定为47—105ka或许是合理的。但洞穴地点骨化石铀系年代总体偏年轻,上述年代范围很可能被低估。本文结果与我们已有研究的广西通天岩、前洞等地点一致,是晚期智人在我国出现比原认为的早得多的又一例证。     

New Luminescence Ages for the Galería Complex Archaeological Site: Resolving Chronological Uncertainties on the Acheulean Record of the Sierra de Atapuerca,Northern Spain

The archaeological karstic infill site of Galería Complex, located within the Atapuerca system (Spain), has produced a large faunal and archaeological record (Homo sp. aff. heidelbergensis fossils and Mode II lithic artefacts) belonging to the Middle Pleistocene. Extended-range luminescence dating techniques, namely post-infrared infrared stimulated luminescence (pIR-IR) dating of K-feldspars and thermally transferred optically stimulated luminescence (TT-OSL) dating of individual quartz grains, were applied to fossil-bearing sediments at Galería. The luminescence dating results are in good agreement with published chronologies derived using alternative radiometric dating methods (i.e., ESR and U-series dating of bracketing speleothems and combined ESR/U-series dating of herbivore teeth), as well as biochronology and palaeoenvironmental reconstructions inferred from proxy records (e.g., pollen data). For the majority of samples dated, however, the new luminescence ages are significantly (∼50%) younger than previously published polymineral thermoluminescence (TL) chronologies, suggesting that the latter may have overestimated the true burial age of the Galería deposits. The luminescence ages obtained indicate that the top of the basal sterile sands (GIb) at Galería have an age of up to ∼370 thousand years (ka), while the lowermost sub-unit containing Mode II Acheulean lithics (base of unit GIIa) was deposited during MIS 9 (mean age = 313±14 ka; n = 4). The overlying units GIIb-GIV, which contain the richest archaeopalaeontological remains, were deposited during late MIS 8 or early MIS 7 (∼240 ka). Galería Complex may be correlative with other Middle Pleistocene sites from Atapuerca, such as Gran Dolina level TD10 and unit TE19 from Sima del Elefante, but the lowermost archaeological horizons are ∼100 ka younger than the hominin-bearing clay breccias at the Sima de los Huesos site. Our results suggest that both pIR-IR and single-grain TT-OSL dating are suitable for resolving Middle Pleistocene chronologies for the Sierra de Atapuerca karstic infill sequences.     

Thermoluminescence dating tests of Pleistocene sediments from uplifted marine shorelines along the southwest coastline of the Calabrian Peninsula (southern Italy)

This paper presents TL age estimates of Pleistocene raised marine terraces from southern Calabria (southern Italy). It focuses on the dating of last interglacial shallow-marine sand deposits, including several Tyrrhenian key reference deposits whose stratigraphic assignment is based on biostratigraphic evidence (presence of a Strombus bubonius fauna) and geochronometric data (amino-acid data calibrated with U/Th dates on coral). The TL age estimates are obtained on alkali feldspar coarse grains using their blue TL emission. They are in good agreement with the IR-OSL age estimates obtained on the same feldspar samples. Our feldspar TL method is tested on two Tyrrhenian key reference sites, Ravagnese and Bovetto, in the Reggio di Calabria area. Their measured TL age estimates (97 ± 11 ka and 100 ± 10 ka) are lower than their estimated geological age (i.e. Oxygen Isotope Substage 5e). The correction for long-term fading suggested by Mejdahl (1988), is tested on these two samples using a lifetime of 446 ka as estimated from both Calabrian and Miocene sand collected within the same area. This correction would yield preliminary TL ages (116 ± 13 ka and 116 ± 12 ka) that are in better agreement with the expected geological age. The application of our TL method to paleoshorelines lying below the Tyrrhenian reference shoreline of Ravagnese-Bovetto, yields stratigraphically consistent TL age estimates. The TL method is also applied to two supposedly pre-last interglacial paleoshorelines which are geomorphologically older than the Tyrrhenian reference shorelines. They remain however chronologically undifferentiated, both by the TL and the amino-acid methods. Finally, the preliminary feldspar TL results obtained on the Miocene and the Calabrian sand deposits (> 1 Ma), suggest that our feldspar TL method is limited, in the SW Calabrian area, to about 200 ka.     

北京猿人第一个头盖骨及其遗址堆积层年代的电子自旋共振测年研究

裴文中教授在60年前发现的北京猿人第一个头盖骨埋藏的确切年代至今没有获得。本文通过对北京猿人共生的古脊椎动物牙化石进行电子自旋共振(ESR)测年,分别获得了第11层北京猿人第一个头盖骨埋藏的年代为578千年,第8—9层和第3—4层北京猿人埋藏的年代分别为418千年和282千年。依据ESR、U系,TL,FT和古地磁等测年结果,本文推荐了北京猿人洞的洞穴堆积层(周口店组Q_2)年代表供读者参考。     

Models and realities in modern human origins: the African fossil evidence.

The recent application of such chronometric techniques as electron spin resonance (ESR), thermoluminescence (TL), and uranium series dating has had a significant impact on perceptions of modern human origins. Claims for the presence of anatomically modern humans in Africa prior to 100 ka and for the transition leading to modern Africans at an even earlier date have been made, partly based on results of these techniques. However, a careful examination of the pertinent record shows that these claims are not unequivocally supported by the available fossil and chronological evidence.     

A critique of the chronometric evidence for hominid fossils: I. Africa and the Near East 500-50 ka

The chronometric dating evidence for all hominid fossils from Africa and the Near East that have previously been dated to 500-50 ka is critically assessed using the concept of chronometric hygiene, and these dates are revised using Bayesian statistical analyses where possible. Sixteen relevant hominid sites lacking chronometric evidence are briefly discussed. Chronometric evidence from 37 sites is assessed in detail. The dates for many hominid fossils are poorly constrained, with a number dated by comparisons of faunal assemblages-a method that does not have good chronological resolution for much of the last million years. For sites with stratigraphic sequences of dates, it is generally possible to refine the dating, but in some cases, the revised chronology is less precise than previous chronologies. Fossils over 200 ka in age tend to be poorly dated, but for the last 200 kyr, dating is better due to the availability of electron-spin-resonance and thermoluminescence dating. Consideration of the chronologies favored by the proponents of the out-of-Africa and multiregional hypotheses of human evolution shows their selectivity. The chronological assessment of the fossils here is compatible with either hypothesis. If evolutionary schemes that do not rely on the morphology of the hominid fossils to decide the sequence of fossils are to be built, then further dating is required, alongside full publication of existing dates.     

Gamma-ray spectrometric dating of late Homo erectus skulls from Ngandong and Sambungmacan, Central Java, Indonesia

Hominid fossils from Ngandong and Sambungmacan, Central Java, Indonesia, are considered to be the most anatomically derived and youngest representatives of Homo erectus. Nondestructive gamma-ray spectrometric dating of three of these Homo erectus skulls showed that all samples underwent uranium leaching. Nevertheless, we could establish minimum age estimates of around 40ka, with an upper age limit of around 60 to 70ka. This means that the Homo erectus of Java very likely survived the Toba eruption and may have been contemporaneous with the earliest Homo sapiens in Southeast Asia and Australasia.     

High-precision U-series dating of Locality 1 at Zhoukoudian, China

Thermal ionization mass spectrometric(230)Th/(234)U dating has been carried out on intercalated speleothem samples from the limestone cave occupied by Homo erectus at Zhoukoudian, China. The samples were recently collected in proper stratigraphic context after detailed field examinations. The results show that the age of the No. 5 Skull from Layer 3 is >400 ka, possibly in the range of about 400-500 ka, and that the hominid fossils from the lower strata are at least 600 ka and possibly >800 ka, much older than previously thought. The near-equilibrium(230)Th/(234)U ratios and internal consistency of the dates and stratigraphy lend credence to the results and allow us to comment on their important implications for human evolution.     

On the age of Border Cave 5 human mandible

An enamel fragment from the Border Cave 5 specimen was analysed with non-destructive ESR combined with laser ablation ICP-MS for uranium profiling. We obtained an age of 74+/-5 ka which fits exactly into the chronological framework that has been previously established for Border Cave by a variety of dating techniques. The result lays at rest the view that BC5 could be of Iron Age, as was implied by (Journal of Human Evolution, 31 (1996) 499) based on nitrogen contents and infra-red splitting factors.     

旧石器和古人类遗址释光测年技术的可靠性和测年上限

释光测年技术已成为旧石器和古人类遗址,尤其是现代人类遗址,建立年代框架的重要工具之一。这一技术提供了现代人类出现在非洲、亚洲和澳大利亚的最早年代证据。本文简要介绍了释光测年的基本原理,对释光测年的可靠性和上限及所受的影响因素进行了综述。光释光测年的精密度(相对标准误差σ)一般为5%-10%,在理想条件下σ<5%,但是σ>10%的情况也不少见。与大量其他测年方法所获结果的一致性表明,光释光测年技术是可靠的。光释光测年的上限与样品的释光性质及环境剂量率有关,释光可靠年龄最大可达1百万年。对大多数遗址50万年的测年上限是可行的,这个年代范围涵盖了所有的现代人遗址。不同样品或颗粒间的释光性质差异很大,因而它们有不同的测年上限。同一样品中钾长石比石英有更高的测年上限,同一矿物中不同的释光信号对应的测年上限也不同。     

Electron spin resonance dating in paleoanthropology

Many archeological and paleoanthropological sites cannot be dated by well established and common dating techniques such as uranium series (U-series) or argon-argon (⁴⁰Ar/³⁹Ar) because of the lack of materials that are suitable for these techniques. Most sites, however, contain bones and teeth, and the latter can be used to obtain electron spin resonance (ESR) age estimates. The theoretical age range of ESR dating accuracy lies between a few thousand and more than a million years. In practice, continuing uranium accumulation increases the uncertainty of ESR age assessments in such a way that most age assignments beyond 300,000 years are very uncertain.     

Application of U/Th and 40Ar/39Ar Dating to Orgnac 3, a Late Acheulean and Early Middle Palaeolithic Site in Ardèche,France

Refined radio-isotopic dating techniques have been applied to Orgnac 3, a Late Acheulean and Early Middle Palaeolithic site in France. Evidence of Levallois core technology appeared in level 4b in the middle of the sequence, became predominant in the upper horizons, and was best represented in uppermost level 1, making the site one of the oldest examples of Levallois technology. In our dating study, fourteen speleothem samples from levels 7, 6 and 5b, were U/Th-dated. Four pure calcite samples from the speleothem PL1 (levels 5b, 6) yield ages between 265 ± 4 (PL1-3) and 312 ± 15 (PL1-6) thousand years ago (ka). Three samples from the top of a second stalagmite, PL2, yield dates ranging from 288 ± 10 ka (PL2-1) to 298 ± 17 ka (PL2-3). Three samples from the base of PL2 (level 7) yield much younger U/Th dates between 267 and 283 ka. These dates show that the speleothems PL1 and PL2 are contemporaneous and formed during marine isotope stage (MIS) 9 and MIS 8. Volcanic minerals in level 2, the upper sequence, were dated by the ⁴⁰Ar/³⁹Ar method, giving a weighted mean of 302.9 ± 2.5 ka (2σ) and an inverse isochron age of 302.9 ± 5.9 ka (2σ). Both ⁴⁰Ar/³⁹Ar dating of volcanic sanidines and U/Th dating of relatively pure and dense cave calcites are known to be well established. The first parallel application of the two geochronometers to Orgnac 3 yields generally consistent results, which point to the reliability of the two methods. The difference between their age results is discussed.     

古人类遗址湖北郧西黄龙洞的铀系年代

湖北郧西黄龙洞为近年来发现的晚期智人遗址。本文报道该地点具明确层位意义的洞穴次生碳酸盐岩和骨化石样铀系测年的结果。含文化堆积下伏一局部钙板的年代为约100ka BP, 其中部偏上一局部钙板为约77ka BP, 表层钙板形成于27—57ka BP间。人类化石和石制品出土于文化堆积的底部, 其年代应在57—100ka BP, 并很可能在77—100ka BP间。与人牙化石同层的四枚犀牛牙化石在35—72ka BP间, 与基于次生碳酸盐岩的年代框架没有冲突。本文结果为中国现代人类的早期出现和距今40—100ka BP间有人类活动提供了有力证据。     

The Pech-de-l'Azé I Neandertal child: ESR, uranium-series, and AMS 14C dating of its MTA type B context

The Pech-de-l'Azé I skull and mandible are included in the juvenile Neandertal remains from Europe. However, some preserved features in the cranial skeleton seem to distinguish the specimen from other Neandertal children. Unfortunately, the stratigraphic position and dating of this child has never been clear. Our recent work on unpublished archives show that the Pech-de-l'Azé I Neandertal child was discovered at the bottom of layer 6, attributed to the Mousterian of Acheulean tradition type B. These skull and mandible are the first diagnostic human remains (aside from an isolated tooth) attributed to the Mousterian of Acheulian tradition (MTA) type B. Consequently, we confirm that Neandertals were the makers of this Mousterian industry, which is characterized by unusual high frequencies of Upper Paleolithic type tools, elongated blanks and blades. We were able to date the context of the hominid remains by dating layer 6 and the layers above and beneath it using ESR, coupled ESR/(230)Th/(234)U (coupled ESR/U-series), and AMS (14)C. Coupled ESR/U-series results on 16 mammalian teeth constrain the age of the uppermost layer 7 to 41-58ka, and layer 6 to 37-51ka. The wide spread in each age estimate results mainly from uncertainties in the gamma-dose rate. These ages are concordant with AMS (14)C ages of two bones coming from the top of layer 6, which provide dates of about 41.7-43.6ka cal BP. A combination of stratigraphic arguments and dating results for layers 6 and 7 show that the Neandertal child cannot be older than 51ka or younger than 41ka. The lowermost layer 4 is shown to be older than 43ka by the principle of superposition and ESR dating in the immediately overlying layer 5. This study shows that the MTA type B had been manufactured by Neandertals before the arrival of anatomically modern humans in the local region. Additionally, by providing a firm chronological framework for the specific morphometric the features of Pech-de-l'Azé I Neandertal child, this study is a new step toward the understanding of temporal and spatial changes in the ontogenesis of Neandertals in south-western Europe during oxygen isotope stages 5-3.