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A new vanadyl oxalatophosphate compound, (C10H10N2)[(VO)(HPO4)]2(C2O4), was synthesized via the hydrothermal approach and characterised structurally using single-crystal X-ray diffraction, FT-IR and thermogravimetric analysis. The compound has two-dimensional anionic layers with occupying the interlayer spaces. 相似文献
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Rui-Qin Fang 《Inorganica chimica acta》2006,359(7):2023-2028
Hydrothermal reaction of molybdenum oxide and copper(II) source in the presence of 4,4′-bipyridine (4,4′-bpy) afforded three-dimensional covalent framework [CuII(4,4′-bpy)(MoO4)] (1), while reaction with 1,4-diazoniabicyclo[2,2,2]octane (DABCO) in place of 4,4′-bpy and addition of metal molybdenum resulted in one-dimensional chain-like compound . The copper in 1 is divalent and approximately shows trigonal bipyramidal geometry, while in 2 is monovalent and approximately shows T-shaped geometry. The structure of 1 has a three-dimensional pillar-layered framework constructed from bimetallic {CuMoO4} layers bridged by bifunctional ligand 4,4′-bpy. Interestingly, the {CuMoO4} layer in 1 consists of 16-membered {Cu4Mo4O8} rings and 8-membered {Cu2Mo2O4} rings, different from other reported {CuMoO4} layers. The structure of 2 consists a one-dimensional chain that is attached by peripheral {Cu(HDABCO)}2+ units. The chain is constructed from octamolybdates through common corners. 相似文献
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Chao Tan Nan-Nan Lu Cheng-Kun Wang Dan-Yang Chen Ning-He Sun Hang Lyu Jakob Körbelin Wei-Xing Shi Kohji Fukunaga Ying-Mei Lu Feng Han 《Neuron》2019,101(5):920-937.e13
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