| 高效液相色谱法测定刺五加超临界提取物中异嗪皮啶的含量 |
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| 引用本文： | 李庆勇,祖元刚,付玉杰,郑春英,赵春建.高效液相色谱法测定刺五加超临界提取物中异嗪皮啶的含量[J].植物研究,2004,24(4):460-461. |
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| 作者姓名： | 李庆勇 祖元刚 付玉杰 郑春英 赵春建 |
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| 作者单位： | 东北林业大学森林植物生态学教育部重点实验室, 哈尔滨 150040 |
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| 摘 要： | 用高效液相色谱法在线检测刺五加超临界提取物中异嗪皮啶的含量, 采用ODS 色谱柱, 检测波长为345 nm, 流动相为乙腈/超纯水(v/v)=2/8, 异嗪皮啶加样回收率100.8%, RSD 为2.0%, 该方法简便, 结果准确可靠。
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| 关 键 词： | 刺五加 异嗪皮啶 高效液相色谱法 |
| 收稿时间： | 2004-01-07 |
| 修稿时间： | 2004年1月7日 |
Determination of isofraxidin in the extract by supercritical CO2 from Acanthopanax senticosus by HPLC |
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| LI Qing-Yong,ZU Yuan-Gang,FU Yu-Jie,ZHENG Chun-Ying,ZHAO Chun-Jian.Determination of isofraxidin in the extract by supercritical CO2 from Acanthopanax senticosus by HPLC[J].Bulletin of Botanical Research,2004,24(4):460-461. |
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| Authors: | LI Qing-Yong ZU Yuan-Gang FU Yu-Jie ZHENG Chun-Ying ZHAO Chun-Jian |
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| Institution: | Key Laboratory of Forest Plant Ecology, Ministry of Education, Northeast Forestry University, Harbin 150040 |
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| Abstract: | Established HPLC determination method of isofraxidin from Acanthopanax senticosus by supercritical CO 2, Method: ODS column was used; The detection wave length was at 345 nm; Mobile phase was acetonitrile/ultrapure water(v/v) = 2/8; The recovery of the added sample was 100.8% and RSD was 2.0% This method is simple and the result is reliable. |
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| Keywords: | Acanthopanax senticosus isofraxidin HPLC |
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