| 积雪苷滴丸的TLC鉴别和HPLC法测定积雪草苷的含量 |
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| 引用本文： | 孙丽娟,王仁友,韦博.积雪苷滴丸的TLC鉴别和HPLC法测定积雪草苷的含量[J].中国微生态学杂志,2009,21(8):715-717. |
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| 作者姓名： | 孙丽娟 王仁友 韦博 |
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| 作者单位： | 深圳市泰康制药有限公司,广东,深圳,518110 |
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| 摘 要： | 目的探索建立积雪苷滴丸的鉴别和含量测定的方法。方法TLC法鉴别积雪苷滴丸中积雪草苷和羟基积雪草苷,HPLC法测定积雪草苷的含量。结果TLC法鉴别积雪草苷和羟基积雪草苷结果满意,HPLC法测定积雪草苷的含量,线性范围：y=0.234x＋49.869,r=0.9999,检出线性范围：0.91～45μg,加样回收率为98.9%。结论上述方法准确、专属性强,可作积雪苷滴丸的定性和定量分析方法。
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| 关 键 词： | 积雪草苷 羟基积雪草苷 积雪苷滴丸 TLC HPLC |
Identification of Asiaticoside and Madecassoside by TLC and determination of the contents of Asiaticoside by HPLC in Jixuegan pill |
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| SUN Li-juan,WANG Ren-you,WEI Bo.Identification of Asiaticoside and Madecassoside by TLC and determination of the contents of Asiaticoside by HPLC in Jixuegan pill[J].Chinese Journal of Microecology,2009,21(8):715-717. |
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| Authors: | SUN Li-juan WANG Ren-you WEI Bo |
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| Institution: | ( Shenzhen Taikang Pharmaceutical Co. , LTD,Shenzhen 518110,China) |
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| Abstract: | Objective To establish identification method of Asiaticoside and Madecassoside and determination of the contents of Asiaticoside in Jixuegan pill.Method TLC was selected for Asiaticoside and Madecassoside and HPLC was selected for Asiaticoside.Result The quantitative evaluation of Asiaticoside range of 0.91～45 μg（r=0.9999）,average recovery was 98.9%,respectively.Conclusion The methods is accurate and specific.They can be used for identification and determination of Jixuegan pill. |
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| Keywords: | TLC HPLC |
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