Hydrothermal synthesis and crystal structure of a novel one-dimensional arsenic vanadate decorated with organonitrogen ligand: [H3V3O26(AsO4)4(phen)8(H2O)2] · 2H2O (phen=phenanthroline)期刊界 All Journals 搜尽天下杂志传播学术成果专业期刊搜索期刊信息化学术搜索

Hydrothermal synthesis and crystal structure of a novel one-dimensional arsenic vanadate decorated with organonitrogen ligand: [H₃V₃O₂₆(AsO₄)₄(phen)₈(H₂O)₂] · 2H₂O (phen=phenanthroline)

Authors:	Yu Hou Dongrong Xiao Enbo Wang Yangguang Li Changwen Hu

Affiliation:	^a Department of Chemistry, Institute of Polyoxometalate Chemistry, Northeast Normal University, Changchun Jilin 130024, PR China ^b State Key Laboratory for Structural Chemistry of Unstable and Stable Species, College of Chemistry and Molecular Engineering, Institute of Physical Chemistry, Peking University, Beijing 100871, PR China

Abstract:	A novel organic-inorganic hybrid vanadium arsenate [H₃V₃O₂₆(AsO₄)₄(phen)₈(H₂O)₂] · 2H₂O 1 (phen=phenanthroline) was synthesized by the hydrothermal reaction of V₂O₅, VOSO₄, Na₂HAsO₄ · 7H₂O, phen and water. Its structure was determined by elemental analyses, XPS spectra, EPR spectrum, TG analysis, IR spectrum and single-crystal X-ray diffraction.

Keywords:	Organic-inorganic hybrid Vanadium arsenate Hydrothermal synthesis Crystal structure
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