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藏药镰形棘豆挥发性成分研究(英文)
引用本文:王栋,杨欢,杨光明,楼成华,童丽,蔡宝昌.藏药镰形棘豆挥发性成分研究(英文)[J].天然产物研究与开发,2010,22(4).
作者姓名:王栋  杨欢  杨光明  楼成华  童丽  蔡宝昌
作者单位:1. 南京中医药大学药学院,南京,210046;江苏省中药炮制重点实验室,南京,210029
2. 青海大学医学院藏医药研究中心,西宁,810001
摘    要:本文通过水蒸气蒸馏、超临界CO2萃取和顶空萃取三种方法并结合GC和GC/MS技术分析藏药镰形棘豆(Oxytropis falcate Bunge)中的挥发性成分,共鉴定出58个化合物,分别占71.0%,85.6%和84.5%。烷烃类、黄酮类和醛类化合物为主要挥发性成分。3种方法得到的挥发性成分在保留时间值上具有一定的连续性,能更完全地阐述清楚藏药镰形棘豆的挥发性成分,为进一步开发利用这种药用植物提供科学依据。

关 键 词:镰形棘豆  挥发性成分  水蒸气蒸馏  超临界CO2提取技术  顶空萃取

Volatile Compositions from A Tibetan Medicine:Oxytropis falcate Bunge
WANG Dong,YANG Huan,YANG Guang-ming,LOU Cheng-hua,TONG Li,CAI Bao-chang.Volatile Compositions from A Tibetan Medicine:Oxytropis falcate Bunge[J].Natural Product Research and Development,2010,22(4).
Authors:WANG Dong  YANG Huan  YANG Guang-ming  LOU Cheng-hua  TONG Li  CAI Bao-chang
Abstract:To examine the volatile compositions from Oxytropis falcate Bunge,the volatiles were obtained using water distillation,supercritical CO2 and headspace extraction methods and their chemical compositions were analyzed by GC and GC/MS.58 compounds were identified and the amount of the identified compounds represented for 71.0%,85.6% and 84.5% of all the volatiles,respectively.The main components were paraffin hydrocarbons 30.1% (water distillation),flavonoid compounds 68.5% (supercritical CO2 extraction) and aldehyde compounds 53.8% (headspace extraction).In addition,micromolecular terpenoids,organic acids,esters,aldehydes and nitrogenous compounds were also identified.It suggested that retention times of the volatiles extracted using three methods were consecutive which could provide a comprehensive volatile composition of O.falcate Bunge and a scientific basis for further development and utilization of this medicinal plant.
Keywords:GC/MS  Oxytropis falcate Bunge  volatile compositions  water distillation  supercritical CO2 extraction  headspace extraction  GC/MS
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