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Biological trace-element measurements using synchrotron radiation
Authors:Robert D. Giauque  Joseph M. Jaklevic  Albert C. Thompson
Affiliation:(1) Lawrence Berkeley Laboratory, University of California, 94720 Berkeley, CA
Abstract:The feasibility of performing X-ray fluorescence trace-element determinations at concentrations substantially below the ppm level for biological materials is demonstrated. Conditions for achieving optimum sensitivity were ascertained. Results achieved for five standard reference materials were, in most cases, in excellent agreement with listed values. Minimum detectable limits of 20 ppb were measured for most elements.
Keywords:X-ray fluorescence  trace element determinations  biological analyses  synchrotron radiation  XRF calibration  minimum detectable limits  biological standard reference materials
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