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Isolation and characterization of limonoate and nomilinoate A-ring lactones
Authors:Zukas Audrius A  Breksa Andrew P  Manners Gary D
Affiliation:United States Department of Agriculture, Western Regional Research Center, Agricultural Research Service, 800 Buchanan Street, Albany, CA 94710, USA.
Abstract:
A method combining solid-phase extraction and reversed-phase high-performance liquid chromatography is described for the isolation of two key metabolites in the limonoid biosynthetic pathway critical to citrus quality. Potassium salts of limonoate A-ring lactone and nomilinoate A-ring lactone were isolated from young Chandler pummelo seedlings and characterized on the basis of proton and carbon NMR data.
Keywords:Citrus glandis   Rutaceae   Limonoids   Limonoate A-ring lactone   Nomilinoate A-ring lactone
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