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| 利用GC-MS技术分析三棱挥发油化学成分(英文) | |
| 引用本文： | 朱凤妹,杜彬,李军,高海生,刘长江,辛广.利用GC-MS技术分析三棱挥发油化学成分(英文)[J].天然产物研究与开发,2010,22(2). |
| 作者姓名： | 朱凤妹 杜彬 李军 高海生 刘长江 辛广 |
| 作者单位： | 1. 河北科技师范学院食品工程系,昌黎,066600 2. 河北科技师范学院分析测试中心,昌黎,066600 3. 沈阳农业大学食品学院,沈阳,110161 4. 鞍山师范学院化学系,鞍山,114005 |
| 摘 要： | 本文采用同时蒸馏萃取法(SDE)提取三棱挥发油化学成分,测得三棱挥发油的得率为3.19%.利用气相色谱-质谱(GC-MS)联用方法从三棱挥发油中分离并确认出32种化学成分.用峰面积归一化法通过G1710BA化学站数据处理系统得出各化学成分在挥发油中的百分含量,其中主要成分为3,5,6,7,8,8a-六氢-4,8a-二甲基-6-(11-methylethyenyl)-2(1H)萘酮(12.95%),2,4,6,7,8,8a-六氢-5(1H)-黄酮(10.72%),十氢4a-甲基-1-萘(5.78%),3H-3a,7-甲撑甙菊环烃(5.69%). |
| 关 键 词： | 三棱 挥发性成分 气相色谱.质谱技术 同时蒸馏萃取 |
Analysis of the Chemical Composition of Essential Oil from Rhizoma sparganii by GC-MS Method |
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| ZHU Feng-mei,DU Bin,LI Jun,GAO Hai-sheng,LIU Chang-jiang,XIN Guang.Analysis of the Chemical Composition of Essential Oil from Rhizoma sparganii by GC-MS Method[J].Natural Product Research and Development,2010,22(2). | |
| Authors: | ZHU Feng-mei DU Bin LI Jun GAO Hai-sheng LIU Chang-jiang XIN Guang |
| Institution: | ZHU Feng-mei1,DU Bin2,LI Jun1,GAO Hai-sheng1,LIU Chang-jiang3,XIN Guang4 1Department of Food Engineering,Hebei Normal University of Science & Technology,Changli 066600,China,2Analysis , Testing Center,Changli 066600 China,3Food Science College,Shenyang Agricultural University,Shenyang 110161,4Department of Chemistry,Anshan Normal University,Anshan 114005 |
| Abstract: | The essential oil obtained by simultaneous distillation extraction of Rhizoma sparganii was analyzed by gas chromatography-mass spectrometry(GC-MS).The content of essential oil from Rhizoma sparganii was 3.19%.Among the forty-two constituent,thirty-three components were characterized representing 78.57% of the total component which was detected.The identification of the volatile compounds was confirmed by comparing the retention indices with standard values of authentic samples.The relative content was calc... |
| Keywords: | Rhizoma sparganii volatile components gas chromatography-mass spectrometry simultaneous distillation extraction |
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