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海州常山挥发性成分HS-SPME-GC-MS分析
引用本文:田璞玉,李昌勤,王金梅,康文艺.海州常山挥发性成分HS-SPME-GC-MS分析[J].天然产物研究与开发,2011,23(6):1077-1079.
作者姓名:田璞玉  李昌勤  王金梅  康文艺
作者单位:河南大学天然药物研究所,开封475004;河南大学中药研究所,开封475004
摘    要:本文首次采用顶空固相微萃取和气质联用技术(HS-SPME-GC-MS),分析了海州常山花的挥发性成分.从海州常山花中共鉴定出了27种化合物,占挥发油成分总峰面积的94.10%,主要有烷烃、醛、醇和酸类.其中含量较高的成分有2,6,10,14-四甲基十六烷(17.25%)、棕榈醛(10.57%)、1-辛烯-3-醇(6.7...

关 键 词:固相微萃取  海州常山  挥发性成分

Volatiles in Clerodendron trichotomum Thunbby Head-Space Solid Micro-Extraction Coupled with GC-MS
TIAN Pu-yu,LI Chang-qin,WANG Jin-mei,KANG Wen-yi.Volatiles in Clerodendron trichotomum Thunbby Head-Space Solid Micro-Extraction Coupled with GC-MS[J].Natural Product Research and Development,2011,23(6):1077-1079.
Authors:TIAN Pu-yu  LI Chang-qin  WANG Jin-mei  KANG Wen-yi
Institution:TIAN Pu-yu1,2,LI Chang-qin1,WANG Jin-mei1,KANG Wen-yi1,2 1Institute of Natural Products,Henan University,2Pharmaceutical College of Henan University,Kaifeng 475004,China
Abstract:The volatiles in the flowers of Clerodendrum trichotomum Thunb.were analyzed by head-space solid micro-extraction coupled with GC-MS for the first time.Twenty-seven compounds were identified from the C.trichotomum which accounted for 94.10% of the total volatiles.Hydrocarbons,aldehydes,alcohols and acids were the dominant components in the flowers. In addition,2,6,10,14-tetramethylhexadecane(17.25%),hexadecanal(10.57%),1-octen-3-ol(6.78%), benzaldehyde(6.10%) and n-hexadecanoic acid(4.85%) were chief parts ...
Keywords:solid-phase microextraction  Clerodendrum trichotomum Thunb    volatiles  
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