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檵木化学成分研究
引用本文:王刚,刘劲松,李红艳,张凌,刘吉开.檵木化学成分研究[J].天然产物研究与开发,2011,23(2):267-269.
作者姓名:王刚  刘劲松  李红艳  张凌  刘吉开
作者单位:1. 安徽中医学院药学院现代中药安徽省重点实验室,合肥,230031
2. 中国科学院昆明植物研究所,植物化学与西部植物资源持续利用国家重点实验室,昆明,650204
摘    要:采用硅胶柱、ODS和凝胶柱色谱进行分离纯化,通过理化方法和波谱分析进行结构鉴定。从檵木(Loro-petalum chinense(R.Br.)oliver)茎叶中分离并鉴定了六个化合物:植物醇(1)、glycerol 1-(14-methlpentadecano-ate)(2)、methyl-(7R,8R)-4-hydroxy-8′,9′-dinor-4′,7-epoxy-8,3′-neolignan-7′-ate(3)、trans-p-coumaric acid ethylester(4)、落叶松树脂酸(laricinolic acid)(5)、tiliroside(6)。除化合物1外,其余化合物均为首次从檵木中分离得到,化合物2、3首次从该属中分离得到。

关 键 词:檵木  化学成分

Chemical Constituents of Loropetalum chinense
WANG Gang,LIU Jin-song,LI Hong-yan,ZHANG Ling,LIU Ji-kai.Chemical Constituents of Loropetalum chinense[J].Natural Product Research and Development,2011,23(2):267-269.
Authors:WANG Gang  LIU Jin-song  LI Hong-yan  ZHANG Ling  LIU Ji-kai
Institution:WANG Gang1,LIU Jin-song1,LI Hong-yan1,ZHANG Ling2,LIU Ji-kai21Schooll of Materia Madica,Anhui University of Traditional Chinese Medicine,Anhui Key Laboratory of Modernized Chinese Material Medical,Hefei 230031,China,2Kunming Institute of Botany,Chinese Academy of Sciences,State Key Laboratory of Phytochemistry and Plant Resources in West China,Kunming 650204
Abstract:Six compounds were isolated and purified from Loropetalum chinense(R.Br.) oliver by using silica gel,ODS,and Sephadex LH-20 column chromatography,and their structures were determined on the basis of physicochemical properties and spectroscopic analysis.They were identified as trans-phytol(1),glycerol 1-(14-methlpentadecanoate)(2),methyl-(7R,8R)-4-hydroxy-8′,9′-dinor-4′,7-epoxy-8,3′-neolignan-7′-ate(3),trans-p-coumaric acid ethyl ester(4),laricinolic acid(5),tiliroside(6).All of these compounds except 1 were isolated from this plant for the first time.Moreover,it is the first time to report 2 and 3 from the genus Loropetalum.
Keywords:Loropetalum chinense(R  Br  ) oliver  chemical constituents  
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