| 高效液相色谱法检测三羟乙基异氰尿酸酯的纯度 |
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| 引用本文： | 郭卫荣,吴建军.高效液相色谱法检测三羟乙基异氰尿酸酯的纯度[J].氨基酸和生物资源,2010,32(3):73-75. |
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| 作者姓名： | 郭卫荣 吴建军 |
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| 作者单位： | 上海市计量测试技术研究院,理化分析室,上海,201203;上海市计量测试技术研究院,理化分析室,上海,201203 |
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| 摘 要： | 建立了高效液相色谱法定量分析三羟乙基异氰尿酸酯的纯度分析方法。用agilent1100型高效液相色谱仪,CAP-CELL PAK C8(5μm,4.6 mm×250 mm)色谱柱,流动相为乙腈-水,检测波长为210 nm,流速为1.0 ml.min-1,柱温25℃,对三羟乙基异氰尿酸酯纯度进行定量测定。该法重复性好,相对标准偏差为0.15%,标准回收率在99.8%~100.2%,定量结果准确度高。
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| 关 键 词： | 高效液相色谱法 三羟乙基异氰尿酸酯 纯度 |
Purity of 3-Hydroxyethyl Isocyanurate by High Performance Liguid Chromatograph |
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| GUO Wei-rong,WU Jiang-jun.Purity of 3-Hydroxyethyl Isocyanurate by High Performance Liguid Chromatograph[J].Amino Acids & Biotic Resources,2010,32(3):73-75. |
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| Authors: | GUO Wei-rong WU Jiang-jun |
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| Institution: | GUO Wei-rong,WU Jiang-jun(Shanghai Institute of Mesurement and Testing Technology,Shanghai 201203,China) |
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| Abstract: | Purity analysis of 3-hydroxyethyl isocyanurate was established by high performance liquid chromatography with agilent1100,CAPCELL PAK C8(5μm,4.6mm×250 mm)column,mobile phase was acetonitrile-water,detection wavelength was 210nm,flow rate was 1.0 mL·min-1,column temperature was 25℃.The method showed repeatability and relative standard deviation was 0.15%.Standard recoveries were 99.8%-100.2%,quantitative results showed high accuracy. |
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| Keywords: | high performance liguid chromatograph 3-hydroxyethyl isocyanurate purity |
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