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| 东当归化学成分研究及定量分析 | |
| 引用本文： | 刘向前,李丽丽,倪娜,郑礼胜.东当归化学成分研究及定量分析[J].天然产物研究与开发,2011,23(4):693-695. |
| 作者姓名： | 刘向前 李丽丽 倪娜 郑礼胜 |
| 作者单位： | 1. 中南大学制药工程系,长沙410083;湖南中医药大学药学院,长沙410007 2. 中南大学制药工程系,长沙,410083 3. 扬子江药业集团有限公司,泰州,225321 |
| 摘 要： | 从当归属植物东当归的根的乙醇溶液中分离得到了4个化合物,通过理化特性和波谱分析分别鉴定为双(5-甲酰基糠基)醚(bis(5-formylfurfuryl)ether,1)、5-羟甲基糠醛(5-hydroxymethyl-2-furaldehyde,2)、豆甾醇(stigmasterol,3)、十七烷酸(heptadecanoic acid4,)。所有化合物均为首次从该植物中分离得到,其中1为首次从该属植物中分离得到。采用高效液相色谱法对东当归所含该属特征活性成分紫花前胡素进行了定量分析。 |
| 关 键 词： | 当归属 东当归 双(5-甲酰基糠基)醚 高效液相色谱法 紫花前胡素 |
Chemical Constituents and Quantitative Analysis of Angelica acutiloba kitag |
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| LIU Xiang-qian,LI Li-li,NI Na,ZHENG Li-sheng.Chemical Constituents and Quantitative Analysis of Angelica acutiloba kitag[J].Natural Product Research and Development,2011,23(4):693-695. | |
| Authors: | LIU Xiang-qian LI Li-li NI Na ZHENG Li-sheng |
| Institution: | LIU Xiang-qian1,2,LI Li-li1,NI Na3,ZHENG Li-sheng1 1Department of Pharmaceutical Engineering,Central South University,Changsha 410083,China,2College of Pharmacy,Hunan University of Chinese Medicine,Changsha 410007,3Yangtze River Pharmaceutical Group,Taizhou 225321 |
| Abstract: | Four compounds were isolated from the roots of Angelica acutiloba kitag.and their structures were identified as bis(5-formylfurfuryl)ether(1),5-hydroxymethyl-2-furaldehyde(2),stigmasterol(3),heptadecanoic acid(4) by spectroseopic evidences(1H NMR,13C NMR,HR-MS,etc).All the compounds were isolated from this plant for the first time and compounds 1 was obtained from this genus for the first time.The relative contents of decursin which was the special active constituent of Angelica genus were analyzed by HPLC. |
| Keywords: | Angelica Angelica acutiloba kitag bis(5-formylfurfuryl)ether HPLC decursin |
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