Synthesis, spectral and structural studies of novel binuclear Ni(II) complex of salicylaldehyde 3-azacyclothiosemicarbazone |
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| Authors: | Leji Latheef |
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| Affiliation: | Department of Applied Chemistry, Cochin University of Science and Technology, Kochi, 682 022 Kerala, India |
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| Abstract: | ![]()
A novel binuclear Ni(II) complex of salicylaldehyde 3-azacyclothiosemicarbazone (H2L) has been synthesized and characterized by elemental analysis, IR and UV-Vis spectroscopy. The single crystal X-ray structure of the complex shows that bridging occurs through thiolato sulfur and phenolic oxygen atoms. Nickel centers in the complex have square planar and octahedral geometries. |
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| Keywords: | Ni(II) complex Salicylaldehyde Thiosemicarbazone Crystal structure 1,10-Phenanthroline |
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