|
|||||
|
|
| 南海海绵Pachychalinasp.化学成份的研究 | |
| 引用本文： | 肖定军 吴厚铭. 南海海绵Pachychalinasp.化学成份的研究[J]. 天然产物研究与开发, 1997, 9(3): 1-4 |
| 作者姓名： | 肖定军 吴厚铭 |
| 作者单位： | 中国科学院广州化学研究所，中国科学院广州化学研究所，中国科学院上海有机化学研究所 广州 510650，广州 510650，上海 200032 |
| 基金项目： | 国家自然科学基金，中科院上海有机化学研究所生命有机国家重点实验室资助 |
| 摘 要： | 从中国南海海绵Pachychalina sp.正丁醇可溶部分获得了5个化合物,通过UV,IR,~1H-NMR,~(13)C-NMR,MS,~1H-~1HDQFCOSY等实验确定了它们的结构分别是:对羟基苯醋酸甲酯(1),胸腺嘧啶(2),尿嘧啶(3),胸腺嘧啶脱氧核苷(4)和尿嘧啶脱氧核苷(5)。其中化合物(1)是首次从我国南海海洋生物中获得;化合物(5)则是首次从海绵中分离得到的天然产物。 |
| 关 键 词： | 海绵 化学成分 分离提纯 结构鉴定 |
A STUDY ON CHEMICAL CONSTITUENTS OF THE SOUTH CHINA SEA MARINE SPONGE PACHYCHALINA SP. |
|
| Xiao Dingjun,Deng Songzhi. A STUDY ON CHEMICAL CONSTITUENTS OF THE SOUTH CHINA SEA MARINE SPONGE PACHYCHALINA SP.[J]. Natural Product Research and Development, 1997, 9(3): 1-4 | |
| Authors: | Xiao Dingjun Deng Songzhi |
| Abstract: | Five known compounds were isolated from the marine sponge Pachychalina sp. of South China Sea. The crud ethanol extract was partitioned between ethyl acetate and water,then between n- butanol and water. The butanol fraction was chromatographed on silica gel column to obtain Methyl p-hydroxyphenylacetate (1) , thymine (2) , uracil (3 ) , thymidine (4 ) and 2'-deoxyurdine (5). Their structures were determined by UV, IR,MS,1H-NMR,13C-NMR and H-1HDQFCOSY data. It is first reported compound(1) isolated from Chinese marine organisms,and Compoud(5) isolated from marine sponge. |
| Keywords: | marine sponge chemical constituent isolation structure determination |
| 本文献已被 CNKI 维普 等数据库收录！ | |