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| 蟾蜍甾烯14β-artebufogenin的核磁共振光谱信号全归属 | |
| 引用本文： | 乔莉,裴月湖,贾继明,宋剑,孟作环.蟾蜍甾烯14β-artebufogenin的核磁共振光谱信号全归属[J].天然产物研究与开发,2012,24(5):624-626. |
| 作者姓名： | 乔莉 裴月湖 贾继明 宋剑 孟作环 |
| 作者单位： | 1. 石家庄以岭医药研究院,石家庄050035;沈阳药科大学中药学院,沈阳110016 2. 沈阳药科大学中药学院,沈阳,110016 3. 石家庄以岭医药研究院,石家庄,050035 |
| 基金项目： | This research project was supported by the National Key Scientific and Technological Project in 11th Five-year Plan(2009ZX09102-140) |
| 摘 要： | 本论文利用柱色谱法从中药蟾酥中分离得到一个蟾蜍甾烯化合物,利用二维核磁共振和其它化学及光谱学手段对其结构进行了鉴定,并首次给出了其完整的核磁信号归属. |
| 关 键 词： | 蟾酥 蟾蜍甾烯 1H和13C核磁共振 14β-artebufogenin 二维核磁共振 |
Complete NMR Spectral Assignments of Bufadienolide 14β-Artebufogenin |
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| QIAO Li , PEI Yue-hu , JIA Ji-ming , SONG Jian , MENG Zuo-huan.Complete NMR Spectral Assignments of Bufadienolide 14β-Artebufogenin[J].Natural Product Research and Development,2012,24(5):624-626. | |
| Authors: | QIAO Li PEI Yue-hu JIA Ji-ming SONG Jian MENG Zuo-huan |
| Institution: | 1Yiling Medical Research Academy,Shijiazhuang 050035,China;2School of Traditional Chinese Materia Medica,Shenyang Pharmaceutical University,Shenyang 110016,China |
| Abstract: | In this paper we studied the chemical constituents from traditional Chinese drug Chansu.One bufadienolide which named as 14β-artebufogenin was separated by column chromatography and its structure was elucidated based on chemical and spectral analysis.The complete assignments of its 1H and 13C NMR spectral signals were assisted by 2D NMR spectra methods. |
| Keywords: | Chansu bufadienolides 1H and 13C NMR 14β-artebufogenin 2D NMR |
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